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論文

Laser beam direct energy deposition of graded austenitic-to-martensitic steel junctions compared to dissimilar electron beam welding

Villaret, F.*; Boulnat, X.*; Aubry, P.*; 矢野 康英; 大塚 智史; Fabregue, D.*; de Carlan, Y.*

Materials Science & Engineering A, 824, p.141794_1 - 141794_10, 2021/09

 被引用回数:3 パーセンタイル:24.75(Nanoscience & Nanotechnology)

This article presents the Laser Beam Direct Energy Deposition (DED-LBD) process as a method to build a graded austenitic-to-martensitic steel junction. Builds were obtained by varying the ratio of the two powders during DED-LB processing. Samples with gradual transitions were successfully obtained using a high dilution rate from one layer to the next. Long austenitic grains are observed on 316L side while martensitic grains are observed on Fe-9Cr-1Mo side. In the transition zone, the microstructure is mainly martensitic. Characterizations were performed after building and after a tempering heat treatment at630$$^{circ}$$C during 8h and compared to dissimilar Electron Beam (EB) welds. Before heat treatment, the DBD-LB graded area has high hardness due to fresh martensite formed during building. Tempering heat treatment reduces this hardness to 300 Hv. EDS measurements indicate that the chemical gradient between 316L and Fe-9Cr-1Mo obtained by DED-LB is smoother than the chemical change obtained in EB welds. Microstructures in DED-LB samples are quite different from those obtained by EB welding. Hardness values in DMD-LB samples and in welds are similar; the weld metal and the Fe-9Cr-1Mo HAZ are relatively hard after welding because of fresh martensite, as found in the DED-LB transition zone; both are softened by the tempering heat treatment. Both welds were overmatched at 20, 400 and 550$$^{circ}$$C.

論文

Neutron-irradiation effects on charpy impact and tensile properties of low-and high-purity Fe-9Cr alloys

菱沼 章道; 若井 栄一; 高木 清一*; 安彦 兼次*

Proc. of Int. Conf. on Ultra-high purity base metals (UHPM-98), p.27 - 33, 1998/00

高クロム合金は、耐食性、高温強度特性に優れていることから、その合金の開発が待たれている。そのためには、この合金の最大の欠点である脆さを克服する必要がある。本研究では、高純度化の観点から脆さを克服すること及び不純物に大きく影響される照射挙動を明らかにし原子力材料としての開発基盤を確立することの一環として、純度の異なるFe-9Cr合金のシャルピー及び引張特性に及ぼす中性子照射効果を調べた。シャルピー試験によるDBTTの変化に関しては、高純度材の照射による上昇が大きく、また、引張強度の上昇も大きいことがわかった。この原因は照射中に生じる転移ループと析出物の挙動とも密接に関連している。

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